With the blessing of my Parents, teachers and well-wisher herewith I present the book entitled "Practical Pharmaceutical Analysis" to active academics and students, especially for B.Pharma. This book is written as per the new B.Pharma course as per PCI regulation.The main purpose of the subject is to understand about Practical aspects and how it can be applied to industry and thus to improve the quality of the products. The subject covers the complete information about methodologies for Chemical and Instrumental analysis and application. The information provided in this book has been collected from a different journal, websites, official compendia like IP, BP and USP.The contents are well merged from different resources in simplified language. It will be helpful for the student to understand the basics of in a single platform and also for their early professional carrier from an industry point of view.